Biomolecular Nuclear Magnetic Resonance Facility

Conference Proceedings

L. Serventi, J. Sachleben, and Y. Vodovotz. “Effect of soy addition on microwavable parbaked frozen doughs,” in: Magnetic Resonance in Food Science: Challenges in a Changing World, M. Guojonsdottir, P. Belton and G. Webb (Eds.) Royal Society of Chemistry, UK. 2009, 115-125.

Reviews

A.K. Srivastava, J. M. Pittman, J. Zerweck, B. S. Venkata, P. C. Moore, J. R. Sachleben, S. C. Meredith. “β-Amyloid aggregation and heterogeneous nucleation.” Protein Science. 28 (2019) 1567-1581. DOI: 10.1002/pro.3674

Publications

  1. Mustafi, J. Sachleben, G. Wells, M. Makinen. “Structure and Conformation of Spin-Labeled Amino Acids in Frozen Solutions Determined by Electron Nuclear Double Resonance. 1. Methyl N-(2,2,5,5-Tetramethyl-1-oxypyrrolinyl-3-carbonyl)-L-alanate, a Molecule with a Single Preferred Conformation” Journal of the American Chemical Society. 112. (1990) 2558.
  2. Llor, Z. Olejniczak, J. Sachleben, A. Pines. “Scaling and Time Reversal of Spin Couplings in Zero-Field NMR.” Physical Review Letters. 67. (1991) 1989. 
  3. R. Sachleben, E.W. Wooten, L. Emsley, A. Pines, V. Colvin, A.P. Alivisatos. “NMR Studies of the Surface Structure and Dynamics of Semiconductor Nanocrystals.” Chemical Physics Letters. 198. (1992) 431.
  4. Goldman, P. Grandinetti, A. Llor, Z. Olejniczak, J. Sachleben. J. Zwanziger. “Theoretical Aspects of Higher Order Truncations.” Journal of Chemical Physics. 97. (1992) 8947.
  5. Joseph R. Sachleben, Stefano Caldarelli, Lyndon Emsley. “The Effect of Spin Decoupling on Lineshapes in Solid-State Nuclear Magnetic Resonance.” Journal of Chemical Physics. 104. (1996) 2518.
  6. Ales Medek, Joseph R. Sachleben, Peter Beverwyk, Lucio Frydman. “Multi-Rank NMR Studies of Half-Integer Quadrupoles in Solids by Dynamic-Angle Correlation Spectroscopy.” Journal of Chemical Physics. 104.(1996) 5374.
  7. R. Sachleben, V. Frydman, L. Frydman. “Dipolar Determinations in Solids using Relaxation-Assisted NMR Recoupling.” Journal of the American Chemical Society. 118. (1996) 9786.
  8. Joseph R. Sachleben, Lucio Frydman. “Orientational Alignment in Solids from Bidmensional Isotropic-Anisotropic NMR spectroscopy: Applications to the analysis of Aramide Fibers.” Solid-State NMR. 7. (1997) 301.
  9. R. Sachleben, V.L. Colvin, L. Emsley, E.W. Wooten, A. P. Alivisatos. “Solution State NMR Studies of the Structure and Surface Dynamics of Semiconductor Nanocrystals.” Journal of Physical Chemistry B. 102. (1998) 10117.
  10. Susan E. Latturner, Joseph Sachleben, Bo B. Iversen, Jonathan Hanson, Galen D. Stucky. “Covalent Guest-Framework Interactions in Heavy Metal Sodalites: Structure and Properties of Thallium and Silver Sodalite.” Journal of Physical Chemistry B. 103 (1999) 7135.
  11. T. Chien, X.Xu, J.H. Kim, J. Sachleben, J.S. Speck, F.F. Lange. “Electrical Characterization of BaTiO3Heteroepitaxial Thin Films by Hydrothermal Synthesis” Journal of Materials Research. 14 (1999) 3330.
  12. T. Chien, J. Sachleben, J.H. Kim, J.S. Speck, F.F. Lange. “Synthesis and Characterization of PbTiO3Powders and Heteroepitaxial Thin Films by Hydrothermal Synthesis.” Journal of Materials Research. 14 (1999) 3303.
  13. Joseph R. Sachleben, Peter Beverwyk, Lucio Frydman. “Multidimensional Dipolar Exchange-Assisted Recoupling Measurements in Solid-State NMR” Journal of Magnetic Resonance. 144 (2000) 330.
  14. T. Kwak, S. Prasad, Z. Yao, P.J. Grandinetti, J. R. Sachleben, L. Emsley. “Enhanced Sensitivity in RIACT/MQ-MAS NMR Experiments Using Rotor Assisted Polarization Transfer.” Journal of Magnetic Resonance, 150 (2001) 71.
  15. Dria, J. R. Sachleben, P.G. Hatcher. “Solid-State 13C NMR of Humic Acids at High Magnetic Field Strengths: The Case for High Spinning Frequencies and Advanced Cross-Polarization and Decoupling Techniques.” Journal of Environmental Quality. 31 (2002) 393.
  16. Vodovotz, E. Vittadini, J. R. Sachleben. “Use of 1H Nuclear Magnetic Cross Relaxation Spectroscopy to Probe the Changes in Bread and its Components upon Aging.” Carbohydrate Research, 337 (2002) 147.
  17. Michael A. Coutant, Joseph R. Sachleben, Prabir K. Dutta. “Effect of Rotational Mobility on Photoelectron Transfer: Comparison of Two Zeolite Topologies.” Journal of Physical Chemistry B. 107 (2003) 11000.
  18. Joseph R. Sachleben, Benny Chefetz, Ashish Deshmukh, Patrick G. Hatcher. “Solid-State NMR Characterization of Pyrene-Cuticular Matter Interactions.” Environmental Science and Technology. 38 (2004) 4369.
  19. Joseph R. Sachleben, Janet Gaba, Lyndon Emsley. “Floquet-van Vleck Analysis of Heteronuclear Spin Decoupling in Solids: The Effect of Spinning and Decoupling Sidebands on the Spectrum.” Solid-State Nuclear Magnetic Resonance, 29 (2006) 30.
  20. Joseph R. Sachleben. “Bayesian and Information Theory Analysis of MAS Sideband Patterns in Spin 1/2 Systems.” Journal of Magnetic Resonance, 183 (2006) 123.
  21. Segolene Laage, Joseph R. Sachleben, Stefan Steuernagel, Roberta Pierattelli, Guido Pintacuda, Lyndon Emsley. “Fast Acquisition of Multi-Dimensional Spectra in Solid-State NMR Enabled by Ultra-fast MAS.” Journal of Magnetic Resonance, 196 (2009) 133.
  22. Joseph R. Sachleben, Craig McElroy, Paul Gollnick, Mark Foster. “Mechanism of pH-dependent gene regulation by amino-terminus-mediated homooligomerization of Bacillus subtilis anti –trp RNA-binding attenuation protein.” Proceedings of the National Academy of Sciences USA, 107 (2010) 15385.
  23. Adam L. Cloe, Joseph P. R. O. Orgel, Joseph R. Sachleben, Robert Tycko, Stephen C. Meredith. “The Japanese Mutant Aβ (ΔE22-Aβ1–39) Forms Fibrils Instantaneously, with Low-Thioflavin T Fluorescence Seeding of Wild-Type Aβ1–40 into Atypical Fibrils by ΔE22-Aβ1–39.” 50 (2011) 2026-2039.
  24. Luca Serventi, Joseph R. Sachleben, Yael Vodovotz. “Effect of soy addition on microwavable pocket-type flat doughs.” Journal of Food Science. 76 (2011) E392-E398.
  25. Luca Serventi, Joseph Sachleben, Yael Vodovotz. “Soy addition improves the texture of microwavable par-baked pocket-type flat doughs.” Journal of Thermal Analysis and Calorimetry. 106 (2011) 117-121.
  26. Raymond E. Hulse, Joseph R. Sachleben, Po-Chao Wen, Mahmoud Moradi, Emad Tajkhorshid, Eduardo Perozo. “Conformational Dynamics at the Inner Gate of KcsA During Activation.” Biochemistry. 53 (2014)2557-59. DOI: 10.1021/bi500168u.
  27. Joseph R. Sachleben, Ruiyang Yi, Paul Volden, Suzanne Conzen. “Determining Fatty Acid Compositon of Metabolomic Samples by 1H NMR Spectroscopy.” Journal of Biomolecular NMR. 59 (2014) 161-173. DOI: 10.1007/s10858-014-9836-0.
  28. Aparajita H Chourasia,Kristin Tracy, Casey Frankenberger, Michelle L Boland, Marina N Sharifi, Lauren E Drake, Joseph R Sachleben, John M Asara, Jason W Locasale, Gregory S Karczmar, Kay F Macleod. “Mitophagy defects arising from BNip3 loss promote mammary tumor progression to metastasis.” EMBO Reports. 16(2015) 1145-1163. DOI: 10.15252/embr.201540759.
  29. Katherine I. Zhou,Marc Parisien, Qing Dai, Nian Liu, Luda Diatchenko, Joseph R. Sachleben, Tao Pan. “N6-methyladenosine modification in a long non-coding RNA hairpin predisposes its conformation to protein binding.” Journal of Molecular Biology. 428(2016) 822-33. DOI:10.1016/j.jmb.2015.08.021 
  30. R. Sachleben, A. N. Adhikari, G. Gawlak, R.J. Hoey, G. Liu, A. Joachimiak, G. T. Montelione, T. R Sosnick, and S. Koide. “Aromatic Claw: A new fold with high aromatic content that avoids structural prediction.”Protein Science. 26(2017) 208-217. DOI: 10.1002/pro.3069.
  31. Siyi GuJoseph R. Sachleben, Christopher T. Boughter, Wioletta I. Nawrocka, Marta T. Borowska, Jeffrey T. Tarrasch, Georgios Skiniotis, Benoît Roux, and Erin J. Adams. “Phosphoantigen-induced conformational change of butyrophilin 3A1 (BTN3A1) and its implication on Vγ9Vδ2 T cell activation.” Proceedings of the National Academy of Sciences USA, 114 (2017) E7311–E7320. DOI: 10.1073/pnas.1707547114.
  32. Dianning He, Devkumar Mustafi, Xiaobing Fan, Sully Fernandez, Erica Markiewicz, Marta Zamora, Jeffrey Mueller, Joseph R. Sachleben, Matthew J. Brady, Suzanne D. Conzen, Gregory S. Karczmar. “Magnetic resonance spectroscopy detects differential lipid composition in mammary glands on low fat, high animal fat versus high fructose diets.” PLoS ONE, 13 (2018) e0190929.
  33. Justin L. Luebke, Daniel S. Eaton, Joseph R. Sachleben, Sean Crosson. “Allosteric control of a bacterial stress response system by an anti-sigma factor.” Molecular Microbiology. 107 (2018) 164-179.
  34. Larry House, Michael J. Seminerio, Snezana Mirkov, Jacqueline Ramirez, Maxwell Skor, Joseph R. Sachleben, Masis Isikbay, Hari Singhal, Geoffrey L. Greene, Donald Vander Griend, Suzanne D. Conzen, Mark J. Ratain. “Metabolism of megestrol acetate in vitro and the role of oxidative metabolites.” XenoBiotica, 48 (2018) 973-983. DOI: 10.1080/00498254.2017.1386335.
  35. Jonathan Zerweck, Bharat Somireddy Venkata, Jay M. Pittman, Atul K. Srivastava, Patrick C. Moore, Joseph R. Sachleben, Gopal Thinakaran, Stephen C. Meredith. “A versatile method for producing labeled or unlabeled Aβ55, Aβ40, and other β-amyloid family peptides.” Protein Expression and Purification. 162 (2019) 72-82. https://doi.org/10.1016/j.pep.2019.04.006
  36. Laura M. L. Hawk, Jay M. Pittman, Patrick C. Moore, Atul K. Srivastava, Jonathan Zerweck, Joshua T. B. Williams, Andrew J. Hawk, Joseph R. Sachleben, Stephen C. Meredith. “β-Amyloid Model Core Peptides: Effects of Hydrophobes and Disulfides.” Protein Science. 29 (2020) 527-541.